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* PDF α Ͻñ ٶϴ. |
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1994 / ȣ: V.6,no.2,Jun |
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(II) - Ǻ ó ȭ Ȳȿ Ͽ- |
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A Study on the Crystallinity in Silk Fibers(II) -Crystallization in Silk Fibroin by Acid Treatment and Its Photoyellowing Reduction Effect- |
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(λ꿩 ΰ) ּö (λб Ƿа) |
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24 ~ 29 : 6 |
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Korean |
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In order to investigate the crystallization in silk fibroin induced by acid treatment and its photo-yellowing reduction effect. silk fibroin were immersed in PH 3.5~4.0 sulfuric acid and 0.01N hydro-chloric acid at 2, and the changes of crystallinity were measured by infrared spectroscopy, X-ray diffraction. Yellowness index caused by UV irradiation were also observed. The results are as follows : 1. -form transition occurs when the silk fibroin are immersed at 2 in pH 3.5~4.0 sulfuric acid and 0.01N hydro-chloric acid. Formation of new hydrogenbond in molecules on the amorphous region induced -form structure, and increased crystallinity. 2. Crystallization owing to -form transition reduced the initial yellowness index by ultraviolet irradiation.
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