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1996 / ȣ: V.8,no.2,Apr |
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Poly(4,4\\\'-diphenyl ether pyromellitamic acid) ̵̹ȭ |
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Imidization of Poly(4,4\\\'-diphenyl ether pyromellitamic acid |
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Ahn, Young Moo (Dept. of Clothing and Textiles, Hansung Univ., Seoul, Korea) |
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Ahn, Young Moo (Dept. of Clothing and Textiles, Hansung Univ., Seoul, Korea) |
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Ahn, Young Moo (Dept. of Clothing and Textiles, Hansung Univ., Seoul, Korea) |
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Ahn, Young Moo (Dept. of Clothing and Textiles, Hansung Univ., Seoul, Korea) |
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49 ~ 55 : 7 |
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Korean |
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Poly(4, 4\\\'-diphenyl ether pyromellitamic acid) was prepared from pyromellitic anhydride with 4, 4\\\'-diamino diphenyl ether by means of low-temperature solution polymeriztion. The reation was exothermic and very fast when carried out at room temperature. The synthesized poly(4, 4\\\'-diphenyl ether pyromellitamic acid) was converted to poly(4, 4\\\'-diphenyl ether pyromellitimide) by thermal dehydrocyclization. FTIR analysis was widely used as a means of determining the course of imidization from intensity of characteristic bands of the imide ring at and . The density of poly(4, 4\\\'-diphenyl ether pyromellitimide) was higher than poly(4, 4\\\'-diphenyl ether pyromellitamic acid) indicating the greater crystallinity, perhaps because of the reduction of molar volume of polymers |
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